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Critical Reviews in Anal. Chem.
Lead Analysis: Past and Present
Sublime Lead: A Biography of a 5000 Year Toxic Love Affair
Raymond Lully, 1235 A.D.
Take two to three pounds of the juice of the Lunaria, add a solution of lead, alum, salpetre, sal ammoniac, silver-litharge, quick-silver sublimate, vinegar and ginger, then distil and calcinate. This powder is then thickened with a silver solution into paste. One part in a hundred of this paste, heated on a copper plate, could theoretically turn tin, lead, or quicksilver into silver at a ratio of one to a hundred parts.
Mitchell, 1848 A.D.: An Early Analytical Text
“[The suspected material] is to be acted on with dilute nitric acid, and the resulting liquid filtered. If the addition of dilute sulphuric acid to the filtered liquid produce a white, if chromate of potash a yellow, and , lastly, if sulphuretted hydrogen a black precipitate, the presence of lead is fully determined.”
LECTURE NOTES : text: Skoog, Holler, Crouch, Principles of Instrumental Analysis, 6th Ed
1. Introduction to Lead Lab Lecture ppt 1
lecture pdf
Critical Reviews in Anal. Chem.268-9
Text Chapters 1, 2 &5
2. Statistics Lecture ppt
Statistics Lecture pdf
Reading: Introduction to Statistics and Sampling
3. Filtering and Massaging the Data. ppt
Signal/Noise Lecture pdf
Reading: Signal and Noise Filtering
Instructions Deconvoluting UV-Vis
4. Chemistry of Lead Lecture ppt
Chemistry of Lead Lecture pdf
Critical Reviews in Anal. Chem.269-285
5. Really Basic Optics ppt
Really Basic Optics pdf
Text Chapters 6&7
6. Beer's Laws and It's Implications ppt
Beer's Law and It's Implications pdf
Text Chapter 13
7. UV-Vis Spectroscopies ppt
UV-Vis Spectroscopies pdf
Text Chapters 8&9; 14, 15, and 18
8. IR and NMR Spectroscopy
IR and NMR Spectroscopy pdf
Text Chapters 16,17,19
see this great website
9. GC-MS ppt
GC-MS lecture notes pdf
Text Chapters 26, 27, and 20
EXCEL EXERCISES
1. Data for Box car filtering exercise
2. Fourier Transform Excel Sheet Used In Class
3.Deconvolution of UVVis peaks Used in Class
4. Data for Student FTT exercise
5. Exam I Take Home
6. Excel GC exercise
7. Exam III Instructions and Grading Scheme
8. Information for Exam III on writing exams
LEAD LABORATORIES
** indicates this semester (Spring 2008)
Anal Chem Article on Team Work
0**: Calibrate Your Writing
GFAA Group A Version 1
GFAA Group A Version 2
GFAA Group E Version 1
GFAA Group E Version 2
ICPMS Group B
ICPMS Group C
ICPMS Group D
1**: Population Analysis
Potato Lab correction
Needleman New Eng. J. Med, 1979
2**: S/N and filtering
3: Lead by lead sulphide (turbidity)
4: Lead by lead chromate (gravimetric)
5: Commercial spot tests
6: Electrolytic deposition of PbO2
7**: Anodic Stripping Voltammetry
Liu et al Anal. Chem. 1997
Zelic et al Electrochem Acta 1990
Feldman et al Anal. Chem. 1994
8**: PbS ion selective electrode
Kamata et al Anal. Chem. 1991
9: Titrametric, EDTA with Eriochrome
10: Titrametric, EDTA, UV-Vis detection
11: Lead Iodide determination
12**: Atomic Absorption, Graphite Furnace
Creed et al Env. Sci. Tech. 1992
Marquardt et al Anal. Chem. 1996
13:** Chelation by Dithizone, UV-Vis
Irving et al Anal Chim Acta 1969
14**: Stability of Dithizone by CV
Tomcsanyi Anal Chim Acta 1977
Kassim Inorg Chim Acta 1978
15**. Fluorescence Quenching of CB by Pb
16 Fluorescence of protoporphyrin
Hammond et al Env. Research 1985
17**: IR study of Lead-EDTA chelate
18**: NMR of 207Pb-EDTA complex
19: ICP-MS determination of Pb isotopes
20: Preparative Chromatography for Lead
Manton et al Chem Geol 1988
21: Ion Pair HPLC of Lead EDTA
Shijo et al Anal. Sci. 1993
Liu et al J. Chromatography A 1998
22: GC of Tetraethyl Lead
Brunelto Atomic Spectroscopy 1992
23:** Hot Plate Acid Digestions
24: Sequential Soil Extractions
25: Soil Sampling
26: House Dust Sampling: Wet Wipe
27: House Dust Sampling: Vacuum
28: Water Sampling
29: Blood Sampling
30. Hand Dust Sampling
31. Community Based Problem Solving
Markkula Center for Ethics
32. The Needleman Papers
Ernhardt Ethics & Behavior 1993
Needleman Ethics & Behavior 1993
Scarr Ethics & Behavior 1993
Needleman New Eng J Med 1990
33. The Johnson Controls Case
U.S. District Court
U.S. Supreme Court
SPRING 2008 RAW DATA
1. Potatos
7. Anodic Stripping Voltammetry
8. PbS ISE
12. Flame AA
13. Dithizone UV-Vis
14. Stability of dithizone by CV
15. Fluorescence Quenching of CB by Pb
17. IR Study of Pb-EDTA
18. NMR Study of Pb-EDTA Pb-207
19. GCMS of Pesticides
TOY SCREENING
Article on Screening Toys
Article on Digesting Plastics for Pb
Article on Digesting Toys for Pb
EPA SW-847 3050 Digestion
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